酱香型白酒传统降度工艺探究及风味特征分析OA
Traditional Alcohol Content Reduction Process Exploration and Flavor Characteristics Analysis of Sauce-Flavor Baijiu
以酱香型白酒酒样A(乙醇体积分数53%)为基酒,以浊度及感官评分为评价指标,通过优化降度用水、乙醇体积分数、吸附条件并辅以酒体风味弥补技术,得到较为科学的酱香型白酒降度工艺,并采用气相色谱(GC)、气相色谱-质谱(GC-MS)及常规检测方法对其挥发性风味成分及基本理化指标进行检测.结果表明,酱香型白酒酒样A(乙醇体积分数53%)的降度工艺为酒样中添加反渗透(RO)水使乙醇体积分数降至42%后,选用SX-865澄清剂吸附25 min,抽滤后得到降度酒酒样B(乙醇体积分数42%);添加调味酒融合风味后形成降度酒酒样C(乙醇体积分数42%),酒样C的感官评分为89分,为优级酒.从3种酒样中共检出101种挥发性风味成分,包括酯类35种,醇类19种,醛类、酸类各9种,酮类6种,吡嗪类9种,酚类6种,其他类8种;酒样间各类挥发性成分含量存在差异.结合偏最小二乘判别分析(PLS-DA)发现,相较于酒样B,酒样C更接近酒样A;通过变量投影重要性(VIP)>1、气味活性值(OAV)>1共筛选出乙醛、乙酸乙酯、丙醇、乳酸乙酯、乙缩醛、乙酸、糠醛等10种关键差异挥发性风味化合物.
Using sample A(ethanol volume fraction 53%)of the sauce-flavor(Jiangxiangxing)Baijiu as the base liquor,with turbidity and sensory evaluation score as the evaluation indicators,through optimizing the water for alcohol content reduction,alcohol content,adsorption conditions,and supplemented with the technology by compensating the liquor body flavor,a scientific dilution process for sauce-flavor Baijiu was obtained.The volatile flavor components and basic physicochemical indicators of the sauce-flavor Baijiu were detected by gas chromatography(GC),gas chromatography-mass spectrometry(GC-MS),and conventional detection methods.The results showed that the alcohol content reduction process of sample A(53%)of the sauce-flavor Baijiu was as follows:reverse osmosis(RO)water was added to the sample to reduce the alcohol content to 42%,then using SX-865 clarifier for adsorption 25 min,and after filtration,sample B with reduced alcohol content(42%)was obtained.After adding flavoring liquor to blend the flavor,sample C with reduced alcohol content(42%)was formed.The sensory score of sample C was 89,which was an excellent grade Baijiu.A total of 101 volatile flavor components were detected from the three Baijiu samples,including 35 esters,19 alcohols,9 aldehydes,9 acids,6 ketones,9 pyrazines,6 phenols,and 8 others.There were differences in the content of various volatile components among the Baijiu samples.The partial least squares-discriminant analysis(PLS-DA)found that compared with sample B,sample C was closer to sample A.A total of 10 key different volatile flavor compounds such as acetaldehyde,ethyl acetate,propanol,lactic acid ethyl ester,ethyl acetal,acetic acid,and furfural were selected by variable importance in projection(VIP)>1 and odor activity value(OAV)>1.
许文静;李莹;刘刚德;陈雪雪;顾英婕;胡建锋;路虎;范奇高
贵州习酒股份有限公司,贵州 遵义 564600||贵州省酱香型白酒技术创新中心,贵州 遵义 563000贵州习酒股份有限公司,贵州 遵义 564600||贵州省酱香型白酒技术创新中心,贵州 遵义 563000贵州习酒股份有限公司,贵州 遵义 564600贵州习酒股份有限公司,贵州 遵义 564600||贵州省酱香型白酒技术创新中心,贵州 遵义 563000贵州习酒股份有限公司,贵州 遵义 564600||贵州省酱香型白酒技术创新中心,贵州 遵义 563000贵州习酒股份有限公司,贵州 遵义 564600||贵州省酱香型白酒技术创新中心,贵州 遵义 563000贵州习酒股份有限公司,贵州 遵义 564600||贵州省酱香型白酒技术创新中心,贵州 遵义 563000贵州习酒股份有限公司,贵州 遵义 564600||贵州省酱香型白酒技术创新中心,贵州 遵义 563000
轻工纺织
低度酒酱香型白酒除浊偏最小二乘判别分析基本理化指标挥发性风味成分
low-alcohol Baijiusauce-flavor Baijiuturbidity removalpartial least squares-discriminant analysisbasic physicochemical indicatorvolatile flavor component
《中国酿造》 2026 (4)
78-86,9
贵州省科技攻关计划项目(黔科合支撑[2023]一般343)贵州省技术创新中心项目(黔科合平台JSZX[2025]002)
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