辐射环境残余气体分析仪的研制与应用OA
Development and Application of Residual Gas Analyzer in Radiation Environment
针对同步辐射和核聚变等强辐射真空装置的在线监测需求,常规的残余气体分析仪(Residual gas analyzer,RGA)难以长期稳定工作.本研究构建了分体式抗辐射RGA,并对其结构设计、性能及工程应用开展了系统研究.将四极杆探头等关键器件置于强辐射区,电子学单元通过长电缆实现远程布设,以减轻辐照损伤.按照国家标准(GB/Z 42625-2023)完成仪器性能测试,离子源灵敏度为2.04×10–6 A/Pa,可准确识别H2、He、N2、Kr、Xe和Ar等标准气体组分,各物质特征峰位与理论质荷比一致.开展了 γ 射线静态辐照模拟试验,剂量率为100 Gy/h,探头累积剂量为5250 Gy,电子单元累积剂量为300 Gy.结果表明,随着等效累积辐照服役时长增加,电子倍增器增益持续衰减,即使提高工作电压,其增益也无法恢复至初始性能.利用此仪器开展现场测试,在辐照剂量率为50 Gy/h、真空度为6.27×10–6 Pa的条件下,实时监测通光和关光状态下的气体组分.结果表明,通光时解吸效应显著,腔体内CO和CO2 分压明显升高,切断光束后各气体分压均下降.本研究研制的抗辐射型RGA可稳定监测高辐射环境下的气体,清晰表征光子刺激解吸与电子刺激解吸协同作用,可为同步辐射光源、聚变堆和高能加速器等极端辐射真空装置提供长效在线残余气体监测解决方案.
To satisfy the online monitoring demands of high-radiation vacuum facilities including synchrotron radiation devices and fusion reactors,conventional residual gas analyzers(RGAs)fail to achieve long-term stable operation.A split radiation-hardened RGA was developed and its structural design,performance and engineering applicability were systematically investigated in this work.The quadrupole probe and other core components were placed in high-radiation regions,and the electronic unit was remotely connected through long cables to reduce radiation damage.Performance tests following GB/Z 42625-2023 showed that the ion source sensitivity was 2.04×10–6 A/Pa.The system could recognize H2,He,N2,Kr,Xe,Ar and other standard gases,whose characteristic peaks agreed well with theoretical mass-to-charge ratios.Gamma irradiation experiments were implemented at 100 Gy/h,with cumulative doses of 5250 Gy on the probe and 300 Gy on electronics.The electron multiplier exhibited persistent gain degradation under prolonged irradiation,and elevated working voltage could not restore its original performance.On-site experiments were conducted on a SSRF beamline at 50 Gy/h and 6.27×10–6 Pa for real-time gas monitoring under beam-on and beam-off conditions.Significant desorption occurred during beam operation accompanied by the increased CO and CO2 partial pressures,and all partial pressures decreased after beam cutoff.Experimental results confirmed that the proposed RGA could realize reliable gas measurement under strong radiation and characterize the combined effect of photon-stimulated and electron-stimulated desorption.This work offered a long-duration online residual gas monitoring scheme for synchrotron light sources,fusion reactors and high-energy accelerators.
于佳佳;王新秀;沈辉;庞骏德;任维松;穆辉;赵烨梁;刘俊男;景加荣;侍尉
上海航天裕达科技有限公司,上海 200240||上海卫星装备研究所,上海 200240上海航天裕达科技有限公司,上海 200240上海航天裕达科技有限公司,上海 200240||上海卫星装备研究所,上海 200240上海航天裕达科技有限公司,上海 200240||上海卫星装备研究所,上海 200240上海航天裕达科技有限公司,上海 200240||上海卫星装备研究所,上海 200240上海航天裕达科技有限公司,上海 200240中国科学院上海高等研究院,上海 201210中国科学院上海高等研究院,上海 201210上海航天裕达科技有限公司,上海 200240||上海卫星装备研究所,上海 200240上海航天裕达科技有限公司,上海 200240
残余气体分析仪辐射环境电子倍增器辐照效应真空监测
Residual gas analyzerRadiation environmentElectron multiplierRadiation effectVacuum monitoring
《分析化学》 2026 (9)
1540-1547,8
国家重点研发计划项目(No.2022YFF0707203)资助. Supported by the National Key R&D Program of China(No.2022YFF0707203).
评论