高黏土粉砂岩夹层的压汞−核磁联合评价与甜点识别——以古龙凹陷青一段PⅡ井为例OA
Joint mercury intrusion porosimetry-NMR evaluation and sweet spot identi-fication of high-clay siltstone interlayers:A case study of Well PⅡ in Qing-1 Member,Gulong Depression
松辽盆地古龙凹陷青一段高黏土粉砂岩夹层是页岩油微运移与局部富集的重要载体.受黏土矿物、细喉道以及孔喉连通非均质性共同控制,储层普遍出现"含油而不可动"现象.有必要在同井同岩相条件下厘清孔喉结构与流体可动性的内在关系,建立适用于该类夹层的甜点识别评价标准,规避仅依靠含油性造成的甜点误判.为保障样品可对比性,在 PⅡ 井同井同岩相开展分组配对取样,采用矿物差异指数MDI≤15%作为样品筛选条件;综合开展高压压汞、原状含油二维核磁共振、洗油后饱和模拟地层水−离心核磁共振实验,获取孔喉半径中值r50、分选系数σ、退汞效率、横向弛豫时间T2 截止值、可动流体饱和度等参数;构建复合可动油指数CMOI,综合表征储层含油贡献与流体可动贡献;结合 CT 扫描、扫描电子显微镜(SEM)微观观测,揭示黏土膜状/桥连充填造成细颈喉、孔喉连通受阻的微观机理,解释宏观实验统计规律.高黏土粉砂岩夹层中压汞孔喉参数与核磁可动指标存在显著对应关系:黏土含量升高,r50 减小,可动流体饱和度、CMOI同步降低,T2 几何均值(饱和)随之减小;受黏土束缚水干扰,T2 截止值不适用于样品间横向对比,T2 几何均值(饱和)更适合表征样品可动性差异.基于井段样本分析提出经验甜点判别组合:r50>0.4 μm、可动流体饱和度SMF>40%、CMOI≥20%,在SMF−r50 交会图划分 A~D 4 类评价类型分区,研究样本仅发育 A、B、D 3 类,未见 C 类样品;其中 B 类样品表现为孔喉尺度大但可动性受限,体现"高孔喉≠高可动"的储层特征.受样本数量与取样范围约束,该套判别标准仅适用于 PⅡ井青一段该同岩相井段,后续需扩充样品进一步校验阈值.CMOI与SMF−r50 联合判别方案能够区分含油但动用受限储层,可用于该井段同类夹层样品的甜点识别与评价分类.
[Objective]Continental interlayer-type shale oil in China has become a critical strategic resource for increasing reserves and production.High-clay siltstone interlayers in the First Member of Qingshankou Formation(Qing-1 Member)of Gulong Depression,Songliao Basin,are important carriers of shale-oil micro-migration and local accumulation.Nevertheless,controlled jointly by clay minerals,fine throats,and heterogeneity in pore-throat connectivity,high-clay siltstone interlayers within shale-oil sequences commonly show distinct oil-bearing characteristics but poor fluid mobility.Existing studies lack quantitative coupling relationships between pore-throat parameters derived from high-pressure mercury intrusion porosimetry(MIP)and fluid-mobility indicators obtained from nuclear magnetic resonance(NMR)for such high-clay interlayers,and sweet spot classification still largely relies on empirical judgment.This study targets high-clay siltstone interlayers of the Qing-1 Member in the Gulong Depression,Songliao Basin.Under the constraints of the same well and identical lithofacies,this study aims to clarify the intrinsic relationship between pore-throat structure and fluid mobility,establish a quantitative sweet spot identification criterion,and mitigate misjudgment risks caused by merely using oil-bearing indicators for reservoir evaluation.[Methods]Ten groups of paired core samples from Well PⅡ were collected,and the mineral difference index(MDI)≤15%was used to ensure mineralogical comparability between MIP and NMR subsamples.Integrated laboratory tests,including high-pressure mercury intrusion porosimetry,two-dimensional NMR under original oil-bearing conditions,and centrifugal NMR after oil washing and simulated formation-water saturation,were conducted to obtain key parameters such as median pore-throat radius r50,sorting coefficient σ,mercury withdrawal efficiency,transverse relaxation time T2 cutoff value,movable-fluid saturation SMF,and saturated-state geometric mean of T2.A composite movable-oil index(CMOI=So×SMF/100)was constructed to jointly characterize the contributions of both oil-bearing characteristics and fluid mobility.Based on micro-scale computed tomography(CT)scanning and scanning electron microscopy(SEM)observations,microscopic mechanisms of throat narrowing and pore-throat connectivity impairment induced by clay film coating and bridging infill were revealed to explain the statistical patterns observed in the macroscopic experiments.[Results]For high-clay siltstone interlayers,pore-throat parameters from MIP showed significant correlations with NMR mobility indicators.With increasing clay content,r50 decreased,while SMF,CMOI,and the saturated-state geometric mean of T2 decreased simultaneously.Affected by clay-bound water,the T2 cutoff value was not suitable for cross-sample comparison.Instead,the saturated-state geometric mean of T2 was more suitable for characterizing differences in sample mobility.Based on the analysis of well-interval samples,a empirical sweet spot identification combination was proposed:r50>0.4 μm,SMF>40%and CMOI≥20%.Four evaluation zones(Type A-D)were further defined on the SMF-r50 cross-plot.The samples occurred only in types A,B,and D,with no Type-C samples observed.Type-B samples were characterized by large pore-throat sizes but limited mobility,reflecting the reservoir characteristics of"large pore-throat size does not guarantee high mobility".[Conclusion]Constrained by the sample size and sampling scope,the proposed identification criteria are only applicable to the same-lithofacies interval of the Qing-1 Member within Well PⅡ.Further sample expansion and verification are required for threshold calibration.The joint discrimination scheme combining CMOI and SMF-r50 can effectively distinguish oil-bearing reservoirs with limited mobility,and it can be applied to relative ranking and sweet spot classification of analogous siltstone interlayers within this well interval.
石桓山;胡望水;李涛;李亦博;李姗姗;修静泽
长江大学地球科学学院,武汉 430100||长江大学油气资源与勘探技术教育部重点实验室,武汉 430100长江大学地球科学学院,武汉 430100||长江大学油气资源与勘探技术教育部重点实验室,武汉 430100长江大学地球科学学院,武汉 430100||长江大学油气资源与勘探技术教育部重点实验室,武汉 430100中国石油化工股份有限公司储气库分公司,郑州 450001||中国地质大学(北京)能源学院,北京 100083长江大学地球科学学院,武汉 430100||长江大学油气资源与勘探技术教育部重点实验室,武汉 430100长江大学地球科学学院,武汉 430100||长江大学油气资源与勘探技术教育部重点实验室,武汉 430100
天文与地球科学
古龙凹陷青一段高黏土粉砂岩夹层复合可动油指数甜点识别页岩油压汞−核磁
Qing-1 Member,Gulong Depressionhigh-clay siltstone interlayercomposite movable-oil indexsweet spot identificationshale oilmercury intrusion porosimetry-NMR
《地质科技通报》 2026 (5)
95-111,17
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