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晶体取向对二硅酸锂玻璃陶瓷力学性能的影响OA

Effects of crystallographic orientation on mechanical properties of lithium disilicate glass-ceramics

中文摘要英文摘要

目的:探究晶体定向排布对二硅酸锂玻璃陶瓷微观结构与力学性能的影响.方法:以常规热压铸二硅酸锂玻璃陶瓷为对照组,分别采用常规 ECAP 工艺与改良减径通道 ECAP 工艺制备陶瓷试样.对各组试样纵、横剖面酸蚀后微观形貌观测,测定硬度与断裂韧性,分析裂纹扩展各向异性.结果:ECAP 工艺可有效诱导晶体定向排列,改良减径通道试样的晶体取向一致性更优.相较于常规热压铸组,两种 ECAP 改性试样硬度提升(P<0.05),但断裂韧性降低(P<0.05).结论:改良 ECAP 减径工艺可实现二硅酸锂玻璃陶瓷晶体取向的可控调控,有效提升材料表面硬度,晶体排列取向影响了陶瓷力学性能与裂纹扩展规律.

Objective:To investigate the effects of crystallographic orientation on the microstructure and mechanical properties of lithium disilicate glass-ceramics.Methods:Conventionally hot-pressed lithium disilicate glass-ceramics were set as the control group.Specimens were fabricated via conventional ECAP and modified ECAP with reduced-diameter channels,respectively.Specimens of each group were etched on longitudinal and transverse sections for microscopic morphological ob-servation.Hardness and fracture toughness were tested,and the anisotropy of crack propagation was analyzed.Results:The ECAP technique could effectively induce preferred crystal orientation,and specimens prepared by modified ECAP with re-duced-diameter channels exhibited superior consistency in crystallographic orientation.Compared with the conventional hot-pressed group,both types of ECAP-modified specimens achieved higher hardness(P<0.05),whereas their fracture toughness decreased(P<0.05).Conclusion:The modified ECAP process with reduced-diameter channels enables controllable regula-tion of crystallographic orientation in lithium disilicate glass-ceramics and effectively increases surface hardness.Crystal ori-entation governs the mechanical properties and crack propagation behavior of glass-ceramics.

王雅萱;侯锐;吴婷;张珍珍

空军军医大学基础医学院学员二大队八队 陕西 西安 710032口颌系统重建与再生全国重点实验室,口腔疾病国家临床医学研究中心,陕西省口腔疾病临床医学研究中心,空军军医大学口腔医院颌面外科 陕西 西安 710032武警宁夏总队医院 宁夏 银川 750001口颌系统重建与再生全国重点实验室,口腔疾病国家临床医学研究中心,陕西省口腔医学重点实验室,空军军医大学口腔医院修复科 陕西 西安 710032

医药卫生

二硅酸锂玻璃陶瓷晶体取向等通道转角挤压力学性能

Lithium disilicate glass-ceramicCrystallographic orientationEqual-channel angular pressingMechani-cal properties

《临床口腔医学杂志》 2026 (9)

515-518,4

陕西省卫生健康科研创新能力提升计划重点研发项目(2025YF-10)

10.3969/j.issn.1003-1634.2026.09.002

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