富氧近α钛合金复合片层组织的微织构生成机制和力学行为OA
Micro-texture formation mechanism and mechanical behavior of composite lamellar microstructure in oxygen-enriched near-α titanium alloys
为了解决粉末冶金钛合金富氧时强塑性失衡的难题,采用烧结-热挤压工艺制备出氧含量0.36%(质量分数)的两类α/βt 复合片层组织近α钛合金(880-PE1和880-PE2).采用SEM和TEM分析晶体尺寸和形貌特征,通过XRD宏观织构和EBSD微观织构分析晶体取向信息,结合室温拉伸测试和位错明场像,研究组织与力学性能的关联及变形机制.结果表明:880-PE1无显著微织构,塑性变形时晶界α处诱发裂纹,断后伸长率仅8.9%;880-PE2形成<0001>α平行于挤压方向的微织构.该特殊织构可有效激活锥面<c+a>位错并以波滑移方式运动,引发加工硬化率异常提升,同时促进片层扭曲与晶界协调变形,抑制晶界裂纹萌生.880-PE2抗拉强度达1070 MPa,断后伸长率提升至22.0%,实现强塑性协同改善.
To address the strength-ductility trade-off dilemma of high-oxygen powder metallurgy(PM)titanium alloys,two types of near-α titanium alloys(880-PE1 and 880-PE2)with α/βt composite lamellar microstructure and oxygen mass fraction of 0.36%are fabricated via the combination of sintering and hot extrusion process.The crystal size and morphological characteristics are analyzed by scanning electron microscopy(SEM)and transmission electron microscopy(TEM).The crystallographic orientation features are examined through X-ray diffraction(XRD)macro-texture and electron backscatter diffraction(EBSD)micro-texture analysis.The relationships between microstructure and mechanical properties and deformation mechanisms are studied by combining room-temperature tensile tests and dislocation bright-field imaging observations.The results show that the 880-PE1 specimen exhibits no obvious micro-texture.Cracks initiate at grain boundaries of α phases during plastic deformation,resulting in a low elongation to fracture of only 8.9%.The 880-PE2 specimen develops a micro-texture with the<0001>direction of α grains aligned parallel to the extrusion direction.This unique micro-texture can effectively activate pyramidal<c+a>dislocations,which move via wavy slip and give rise to an extraordinary increase in work-hardening rate.Additionally,lamellar distortion and grain-boundary deformation compatibility are effectively promoted,and the initiation of intergranular cracks is suppressed simultaneously.Ultimate tensile strength of the 880-PE2 specimen reaches 1070 MPa,and the elongation to fracture increases to 22.0%,achieving synergistic improvement of strength-ductility.
张海瑞;牛红志;张德良;张柯柯;陈光
河南科技大学 高温轻合金及应用技术全国重点实验室,河南 洛阳 471023||河南科技大学 材料科学与工程学院,河南 洛阳 471023东北大学 材料科学与工程学院,沈阳 110819东北大学 材料科学与工程学院,沈阳 110819河南科技大学 高温轻合金及应用技术全国重点实验室,河南 洛阳 471023河南科技大学 高温轻合金及应用技术全国重点实验室,河南 洛阳 471023
矿业与冶金
富氧近α钛合金微织构α/βt复合片层组织力学性能加工硬化率
oxygen-enriched near-α titanium alloymicro-textureα/βt composite lamellar microstructuremechanical propertywork-hardening rate
《材料工程》 2026 (8)
31-41,11
国家自然科学青年基金(52301145)
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