石棉检测用折射率浸渍液标准样品的研制OA
Development of Reference Materials for Refractive Index Immersion Liquids Used in Asbestos Detection
针对石棉检测中偏光显微镜法对折射率浸渍液的需求,研制了一套25℃时折射率分别为1.550、1.605、1.630、1.680、1.700 的浸渍液标准样品.选用低毒、稳定的原材料,采用混合配比和硫黄掺杂法精确调控折射率.通过均匀性和稳定性检验,验证了样品在贮存及运输条件下的性能稳定性.联合多家实验室定值,按照标准样品工作导则的要求对定值数据分析处理,获得标准样品的标准值及不确定度.应用测试表明,该系列浸渍液标准样品能有效区分温石棉、透闪石石棉等五种石棉的分散染色特征,符合石棉检测标准要求,填补了石棉检测领域折射率浸渍液标准样品的空白,为石棉鉴定提供了可靠依据.
This study developed a set of refractive index Immersion liquid reference materials for asbestos detection,with refractive indices of 1.550,1.605,1.630,1.680,and 1.700 at 25℃.Low-toxicity and stable raw materials were selected,and the refractive indices were precisely adjusted through mixing and sulfur doping methods.The homogeneity and stability tests confirmed the performance reliability of the samples under storage and transportation conditions.Collaborative characterization by several laboratories,following the guidelines for reference materials,ensured accurate certified values and uncertainty evaluation.Application tests demonstrated that this series of reference materials can effectively distinguish the dispersion staining characteristics of five types of asbestos,including chrysotile and tremolite asbestos,meeting the requirements of asbestos detection standards.This work fills the gap in refractive index Immersion liquid reference materials for asbestos detection and provides a reliable basis for asbestos identification.
宋志堃;郭银祥;昝敏杰;李仔栓
国检测试控股集团北京科技有限公司,北京 100176国检测试控股集团北京科技有限公司,北京 100176国检测试控股集团北京科技有限公司,北京 100176国检测试控股集团北京科技有限公司,北京 100176
天文与地球科学
石棉检测折射率浸渍液标准样品偏光显微镜法不确定度
asbestos detectionrefractive index immersion liquidreference materialpolarized light microscopyuncertainty
《中国非金属矿工业导刊》 2026 (3)
65-69,5
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