粉末热挤出Al-Mn-Mg-Sc-Zr合金的高温拉伸性能及多尺度析出相演化机制OA
High-Temperature Tensile Properties and Multiscale Precipitate Evolution Mechanisms of a Powder Hot-Extruded Al-Mn-Mg-Sc-Zr Alloy
采用气雾化-冷等静压-热挤出工艺制备Al-Mn-Mg-Sc-Zr合金,并研究其室温至300 ℃范围内的高温拉伸性能及多尺度析出相演化规律.结果表明,热挤出态合金形成细小等轴晶组织,基体中弥散分布微米级Al6Mn相和纳米级Al3(Sc,Zr)析出相,同时在晶界处存在不连续分布的MgO颗粒.室温下,合金抗拉强度和屈服强度分别为460.3 MPa和422.8 MPa,伸长率为3.9%;当温度升至200 ℃时获得较优强塑匹配,其抗拉强度、屈服强度和伸长率分别为219.8 MPa、200.2 MPa和23.8%.组织分析表明,高温条件下Al6Mn相发生明显粗化,析出强化作用减弱;而具有L12有序结构并与α-Al基体保持共格界面的Al3(Sc,Zr)相因Sc和Zr扩散速率较低,仍具有较高热稳定性并持续提供强化作用.同时,晶界处存在少量不连续分布的MgO颗粒.多尺度析出相热稳定性的差异是调控该合金高温拉伸行为的主导因素.
Al-Mn-Mg-Sc-Zr alloys were fabricated by gas atomization,cold isostatic pressing,and hot extrusion,and their high-temperature tensile properties and multiscale precipitate evolution from room temperature to 300℃ were investigated.The as-extruded alloy has a fine equiaxed grain structure with micron-sized Al6Mn particles and nanoscale Al3(Sc,Zr)precipitates dispersed in the matrix,whereas discontinuously distributed MgO particles are present along the grain boundaries.At room temperature,the strength of the alloy is high,with an ultimate tensile strength of 460.3 MPa and a yield strength of 422.8 MPa,but the elongation is limited to 3.9%.At 200℃,a favourable strength-ductility balance is obtained,with an ultimate tensile strength of 219.8 MPa,a yield strength of 200.2 MPa,and an elongation of 23.8%.Microstructural analysis indicates that the Al6Mn phase coarsens significantly at elevated temperatures,leading to a weakened strengthening effect.In contrast,the nanoscale Al3(Sc,Zr)precipitates with an ordered L12 structure maintain coherent interfaces with the α-Al matrix and exhibit excellent thermal stability because of the sluggish diffusion of Sc and Zr,thereby continuously contributing to strengthening.Moreover,a small amount of discontinuously distributed MgO particles is present at the grain boundaries.The elevated-temperature tensile behavior of the alloy is governed primarily by the distinct thermal stability of multiscale precipitates.
王蕊;范文新;莫畏;李树奎;余鹏;叶曙龙
深圳北理莫斯科大学材料科学系,广东 深圳 518172||北京理工大学材料学院,北京 100081深圳北理莫斯科大学材料科学系,广东 深圳 518172深圳艾利佳材料科技有限公司,广东 深圳 518107深圳北理莫斯科大学材料科学系,广东 深圳 518172深圳艾利佳材料科技有限公司,广东 深圳 518107深圳北理莫斯科大学材料科学系,广东 深圳 518172
矿业与冶金
Al-Mn-Mg-Sc-Zr合金粉末热挤出高温拉伸多尺度析出相强化机制
Al-Mn-Mg-Sc-Zr alloypowder hot extrusionhigh-temperature tensile propertiesmultiscale precipitatesstrengthening mechanism
《铸造技术》 2026 (5)
498-509,12
深圳市重点产业研发计划(ZDCY20250901101204005)广东省普通高校重点领域专项(2024ZDZX3016)
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