基于相变调控的Ti551钛合金热处理工艺优化OA
Optimization of heat treatment process for Ti551 titanium alloy based on phase transformation regulation
利用光学显微镜、扫描电镜与万能拉伸机,研究了固溶温度、时效温度及冷却速度对 Ti551合金组织与力学性能的影响.固溶温度 900℃时,550~650℃时效温度升高对初生 α相无明显变化,次生 α相片层厚度从0.26 μm增至 0.42 μm;时效温度 550℃时,900~950℃固溶温度升高让初生 α相含量从 45%降至 15%,尺寸细化且形貌由短棒状转为等轴状,次生 α相增厚至 0.72 μm.冷却速度对合金组织起决定性调控作用,炉冷形成单一等轴初生 α相组织,中等冷却速度则细化初生 α相并促进粗大片层次生 α相析出.研究表明,900℃×2 h空冷+550℃×6 h时效的热处理工艺可使 Ti551合金获得最优强韧性匹配,较快冷却速度促使 β组织生成细针状次生α相,经后续时效进一步强化了合金的强塑性匹配效果.
The effects of heat treatment parameters including solution temperature,aging temperature and cooling rate on the microstructure and mechanical properties of a new medium-strength and high-toughness Ti551 alloy were investigated by means of optical microscopy,scanning electron microscopy and universal tensile testing machine.With the same solid solution temperature at 900℃,no obvious changes were observed in the content and size of primary α phase of alloy,while the lamellar thickness of secondary α phase increased from 0.26 μm to 0.42 μm with the aging temperature increasing from 550℃to 650℃.With the same aging temperature of 550℃,the content of the primary α phase de-creased from 45%to 15%as the solution temperature increased from 900℃to 950℃,along with con-tinuous refinement of grains and morphological transformation from short rod-like to equiaxed.The lamellar thickness of the secondary α phase increased accordingly,reaching up to 0.72 μm after alloy subject to solid solution treatment at 950℃.The morphological feature and size of the microstructure are decisively influenced by the cooling rate:an almost single fully equiaxed primary α phase micro-structure is obtained by furnace cooling,whereas the primary α phase is refined and the precipitation of coarse lamellar secondary α phase is promoted by moderate cooling.The results show that optimal strength-toughness combination of the Ti551 alloy is achieved under the composite heat treatment of 900℃×2 h+air cooling,then followed by 550℃×6 h aging,which is closely associated with the regu-latory role of cooling rate.Acicular secondary α phase can be induced in the transformed β microstruc-ture by higher cooling rate,and the alloy's strength-plasticity matching effect is further enhanced by the subsequent aging treatment.
王永锋;申宇波;张宏岭;栾佰峰;周思源;马英杰
重庆大学材料科学与工程学院,重庆 400045||江苏翔云钛合金新材料有限公司,江苏 无锡 214105江苏翔云钛合金新材料有限公司,江苏 无锡 214105江苏翔云钛合金新材料有限公司,江苏 无锡 214105重庆大学材料科学与工程学院,重庆 400045江苏翔云钛合金新材料有限公司,江苏 无锡 214105中国科学院金属研究所师昌绪先进材料创新中心,辽宁 沈阳 110016
矿业与冶金
Ti551钛合金热处理微观组织力学性能
Ti551 titanium alloyheat treatmentmicro-structuremechanical properties
《钢铁钒钛》 2026 (2)
71-77,7
国家重点研发计划(2024YFB3714200).
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