钎焊热循环对GH4169合金组织与力学性能的影响OA
Influence of brazing thermal cycling on microstructure and mechanical properties of GH4169 alloy
为探究不同峰值温度的多次钎焊热循环对GH4169合金组织与性能的影响规律,以GH4169合金为研究对象,系统研究了钎焊热循环工艺对GH4169合金的析出相、晶粒尺寸、拉伸性能及持久性能的影响.结果表明:δ相的析出量随热循环温度的升高呈下降趋势,形态由针状转变为棒状后再转变为颗粒状;在970~1010℃范围内,晶粒尺寸变化不大,而当温度升高至1020℃以上时,晶粒显著长大.抗拉强度和硬度均随热循环温度的升高先增加后降低,并在1010℃时达到峰值,这主要得益于该温度下适量δ相溶解与γ″、γ'强化相的充分析出,而晶粒尺寸并未发生明显粗化;室温冲击韧性在不同的热循环范围具有不同的变化趋势,970~990℃范围内随温度升高而降低,这是由δ相的部分形态由针状转变为棒状所导致;990~1010℃范围内随着温度升高而增加,是由δ相溶解,无强化相析出带消失所导致,而继续增加热循环温度导致冲击韧性下降则是由于晶粒尺寸长大.持久寿命随热循环温度的升高先缩短后延长,在990~1000℃范围内达到最低点,这是由δ相的部分形态由针状转变为棒状,促进微孔形核,降低合金的抗蠕变能力所致.当温度进一步升高至1020℃以上时,γ″强化相大量析出并辅以晶粒显著长大,合金的蠕变性能得以显著改善,但针状δ相含量大幅度降低导致缺口敏感性增强.综合考虑力学性能与缺口敏感性,建议在1010℃左右进行钎焊热循环,可获得较为平衡的强度与持久性能;若服役环境对缺口敏感性要求较高,可选择970~980℃的热循环温度,以降低蠕变失效风险.
To delve into the impacts of multiple brazing thermal cycles at varying peak temperatures on the microstructure and properties of GH4169 alloy,this study conducted a comprehensive examination of how brazing thermal cycle processes influence the precipitates,grain size,tensile properties,and stress-rupture properties of the alloy.The findings reveal that as the thermal cycle temperature rises,the quantity of δ-phase precipitation diminishes,and its morphology undergoes a transformation from needle-like to rod-like and eventually to granular.Within the temperature range of 970-1010℃,the grain size experiences minimal alteration.However,when the temperature surpasses 1020℃,significant grain growth occurs.Both tensile strength and hardness initially ascend and then descend with an increase in the thermal cycle temperature,reaching their peak values at 1010℃.This phenomenon is mainly attributed to the dissolution of an appropriate amount of δ phase and the complete precipitation of γ″ and γ' strengthening phases at this temperature,while the grain size does not show significant coarsening.The room-temperature impact toughness demonstrates distinct trends across different thermal cycle ranges.In the 970-990℃range,it decreases with rising temperature due to the partial transformation of the δ-phase morphology from needle-like to rod-like.In the 990-1010℃range,it increases with temperature as the δ phase dissolves and the strengthening-phase-free zone vanishes.Nevertheless,a further increase in the thermal cycle temperature leads to a reduction in toughness because of grain growth.The stress-rupture life initially declines and then rises with an increase in the thermal cycle temperature,hitting its lowest point in the 990-1000℃range.This is caused by the partial transformation of the δ-phase morphology from needle-like to rod-like,which promotes microvoid nucleation and reduces the alloy's creep resistance.When the temperature further rises above 1020℃,the extensive precipitation of γ″ strengthening phases,along with significant grain growth,substantially enhances the alloy's creep performance.However,the substantial decrease in the needle-like δ-phase content results in increased notch sensitivity.Taking into account both mechanical properties and notch sensitivity,it is recommended to employ brazing thermal cycles around 1010℃to achieve a well-balanced combination of strength and stress-rupture performance.For service environments with higher notch sensitivity requirements,a thermal cycle temperature in the range of 970-980℃can be selected to minimize the risks of creep failure.
王诗洋;张洪宇;刘士伟;武震东;梅寒;张财伟;徐彦强;董佳鹏;郭伟;孙元
中国科学院金属研究所 高温结构材料研究部,沈阳 110016中国科学院金属研究所 高温结构材料研究部,沈阳 110016空装驻辽阳地区军事代表室,沈阳 110000中国科学院金属研究所 高温结构材料研究部,沈阳 110016中国航发沈阳黎明航空发动机有限责任公司,沈阳 110043中国科学院金属研究所 高温结构材料研究部,沈阳 110016中国航发沈阳黎明航空发动机有限责任公司,沈阳 110043中国航发沈阳黎明航空发动机有限责任公司,沈阳 110043北京航空航天大学 航空科学与工程学院,北京 100083中国科学院金属研究所 高温结构材料研究部,沈阳 110016
矿业与冶金
钎焊热循环GH4169显微组织力学性能缺口敏感性
brazing thermal cyclingGH4169microstructuremechanical propertynotch sensitivity
《材料工程》 2026 (3)
113-121,9
辽宁省重点研发计划项目(2024JH2/102400043)国家自然科学基金(52201054)辽宁省自然科学基金(2023010404-JH3/101,2023010697-JH3/107)
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