铜-金刚石复合材料制备方法与性能OA
Preparation method and properties of copper-diamond composites
针对当前电子封装材料热传导性能不足、散热效率低下等问题,利用传统粉末冶金法、搅拌摩擦加工法和放电等离子烧结法三种工艺制备了铜-金刚石复合材料,并对比分析了它们的显微组织结构、相对密度、界面状态以及热导率等性能.结果表明:采用放电等离子烧结法(30 MPa、900 ℃、保温20 min)制备的铜-金刚石复合材料(金刚石体积分数50%)性能最优,金刚石颗粒均匀分布在铜基体上,相对密度97.4%,热导率517.04 W·m-1·K-1,热膨胀系数为6.63×10-6K-1,界面存在厚度不足1 μm的过渡层,结合状态好;传统粉末冶金制备的铜-金刚石复合材料性能次之,搅拌摩擦加工所得材料性能最差.
Addressing the current issues of insufficient thermal conductivity and low heat dissipation efficiency in electronic packaging materials,the copper-diamond composites were prepared with three different methods,namely,traditional powder metallurgy(PM),stirring friction processing(FSP),and spark plasma sintering(SPS),the microstructure,relative density,interfacial state,and thermal conductivity were comparatively analyzed.The results show that the copper-diamond composites with 50%diamond(volume fraction)prepared by SPS under the sintering pressure of 30 MPa at the holding temperature of 900 ℃ for 20 min have the best performance with the diamond particles uniformly distributed on the copper matrix.The relative density,thermal conductivity,and coefficient of thermal expansion of the SPS composites is 97.4%,517.04 W·m-1·K-1,and 6.63×10-6 K-1,respectively,and there is a transition layer with a thickness of less than 1 μm at the interface,which shows good bonding quality.The performance of the copper-diamond composites prepared by PM is the second,and that of the composites prepared by FSP is the worst.
余田亮;陈文革;焦栋茂;牟春浩;马江江
西安理工大学材料科学与工程学院,西安 710048西安理工大学材料科学与工程学院,西安 710048西安理工大学材料科学与工程学院,西安 710048西安理工大学材料科学与工程学院,西安 710048西安理工大学材料科学与工程学院,西安 710048
矿业与冶金
铜-金刚石复合材料粉末冶金搅拌摩擦加工放电等离子烧结制备方法物理性能
copper-diamond compositespowder metallurgystir friction processingspark plasma sinteringpreparation methodphysical properties
《粉末冶金技术》 2026 (1)
25-31,7
陕西省重点研发项目(2023-YF-YBGY-1616)西安市硬科技攻关项目(2024JH-CLYB-0034)西安市碑林区技术研发项目(GX2452)
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