基于多技术联用的金银花酒与基酒成分差异性分析OA
Differential Analysis of Components Between Honeysuckle Wine and Base Wine Based on Multiple Techniques Combination
采用电子鼻、电子舌、离子迁移谱、质谱等多技术联用,分析金银花酒及其基酒的风味特征与化学成分差异.结果显示,电子鼻可辨别酒样气味差异,电子舌可辨别酒样滋味差异,金银花酒的甜味响应值高于基酒,两类酒均无苦涩味.顶空气相色谱-离子迁移谱和顶空固相微萃取-气相色谱-质谱分别检出78种和181种挥发性化合物,超高效液相色谱-四极杆-飞行时间串联质谱检测到138种非挥发性化合物.结果显示,基酒加入金银花浸泡处理后,共计105种化学成分转移至金银花酒中.其中,二氢猕猴桃内酯、丝氨酸及脯氨酸等化合物的转移,提升了金银花酒的甜味特征,使其甜味感官优于基酒.该研究为探究金银花酒的风味形成机制提供了思路,并为金银花酒的生产实践提供了理论依据.
This study employed a multi-technique combination,including electronic nose,electron-ic tongue,ion mobility spectrometry,and mass spectrometry,to analyze the differences in flavor characteristics and chemical compositions between honeysuckle wine and its base wine.Results show that the electronic nose can distinguish the odor differences among wine samples,while the electron-ic tongue can identify the taste differences.The sweetness response value of honeysuckle wine is high-er than that of the base wine,and neither of the two types of wine has a bitter or astringent taste.A to-tal of 78 and 181 volatile compounds are detected by headspace gas chromatography-ion mobility spectrometry(HS-GC-IMS)and headspace solid-phase microextraction-gas chromatography-mass spectrometry(HS-SPME-GC-MS),respectively.Additionally,138 non-volatile compounds are identified using ultra-high performance liquid chromatography-quadrupole-time-of-flight tandem mass spectrometry(HPLC-Q-TOF-MS).After the soaking with honeysuckle,a total of 105 chemi-cal components are transferred to honeysuckle wine.Among them,the transfer of compounds such as dihydroactinidiolide,serine,and proline enhanced the sweetness characteristic of honeysuckle wine,making its sweet sensory property superior to that of the base wine.Overall,this study pro-vides insights into the mechanism of flavor formation in honeysuckle wine and offers a theoretical ba-sis for the production practice of honeysuckle wine.
李玥;卢恒;王晓;付晓;周启红;冯纪君;裴中强;纪文华
齐鲁工业大学(山东省科学院),山东省分析测试中心,天然产物分离提取共性技术创新与应用山东省工程研究中心,山东 济南 250014齐鲁工业大学(山东省科学院),山东省分析测试中心,天然产物分离提取共性技术创新与应用山东省工程研究中心,山东 济南 250014齐鲁工业大学(山东省科学院),山东省分析测试中心,天然产物分离提取共性技术创新与应用山东省工程研究中心,山东 济南 250014山东省金银花行业协会,山东 临沂 273300||山东邑花邑养生物科技有限公司,山东 临沂 273300山东省金银花行业协会,山东 临沂 273300||山东邑花邑养生物科技有限公司,山东 临沂 273300山东省金银花行业协会,山东 临沂 273300||山东邑花邑养生物科技有限公司,山东 临沂 273300山东省金银花行业协会,山东 临沂 273300||山东邑花邑养生物科技有限公司,山东 临沂 273300齐鲁工业大学(山东省科学院),山东省分析测试中心,天然产物分离提取共性技术创新与应用山东省工程研究中心,山东 济南 250014
化学化工
金银花酒基酒顶空气相色谱-离子迁移谱顶空固相微萃取-气相色谱-质谱超高效液相色谱-四极杆-飞行时间串联质谱
honeysuckle winebase wineHS-GC-IMSHS-SPME-GC-MSUPLC-Q-TOF-MS
《分析测试学报》 2026 (3)
573-581,9
国家重点研发计划(2023YFC3503805)中央本级重大增减支项目"名贵中药资源可持续利用能力建设项目"(2060302)
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